ASTM C114-09

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Standard Test Methods for Chemical Analysis of Hydraulic Cement
standard by ASTM International, 02/01/2009

Document Format: PDF

Description

1.1 These test methods cover the chemical analyses of hydraulic cements. Any test methods of demonstrated acceptable precision and bias may be used for analysis of hydraulic cements, including analyses for referee and certification purposes, as explained in Section 3. Specific chemical test methods are provided for ease of reference for those desiring to use them. They are grouped as Reference Test Methods and Alternative Test Methods. The reference test methods are long accepted classical chemical test methods which provide a reasonably well-integrated basic scheme of analysis for hydraulic cements. The alternative test methods generally provide individual determination of specific components and may be used alone or as alternates and determinations within the basic scheme at the option of the analyst and as indicated in the individual method.

1.2 Contents:

Section Subject
2 Referenced Documents
3 Number of Determinations and Permissible Variations
3.1 Referee Analyses
3.2 Optional Analyses
3.3 Performance Requirements for Rapid Test Methods
3.4 Precision and Bias
4 General
4.1 Interferences and Limitations
4.2 Apparatus and Materials
4.3 Reagents
4.4 Sample Preparation
4.5 General Procedures
4.6 Recommended Order for Reporting Analyses
Reference Test Methods
5 Insoluble Residue
6 Silicon Dioxide
6.2 Cements with Insoluble Residue Less Than 1 %
6.3 Cements with Insoluble Residue Greater Than 1 %
7 Ammonium Hydroxide Group
8 Ferric Oxide
9 Phosphorus Pentoxide
10 Titanium Dioxide
11 Zinc Oxide
12 Aluminum Oxide
13 Calcium Oxide
14 Magnesium Oxide
15 Sulfur
15.1 Sulfur Trioxide
15.2 Sulfide
16 Loss On Ignition
16.1 Portland Cement
16.2 Portland Blast-Furnace Slag Cement and Slag Cement
17 Sodium and Potassium Oxides
17.1 Total Alkalis
17.2 Water-Soluble Alkalis
18 Manganic Oxide
19 Chloride
20 Chloroform-Soluble Organic Substances
Alternative Test Methods
21 Calcium Oxide
22 Carbon Dioxide
23 Magnesium Oxide
24 Loss on Ignition
24.1 Portland Blast-Furnace Slag Cement and Slag Cement
25 Titanium Dioxide
26 Phosphorus Pentoxide
27 Manganic Oxide
28 Free Calcium Oxide
Appendices Title
Appendix X1 Example of Determination of Equivalence Point
for the Chloride Determination
Appendix X2 CO2 Determinations in Hydraulic Cements

1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. See 6.3.2.1 and 14.4.1 for specific caution statements.

Product Details

Published:
02/01/2009
Number of Pages:
32
File Size:
1 file , 400 KB
Redline File Size:
2 files , 680 KB
Note:
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